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Germanium is recovered from gerichened vacuumn furnace slag of Shaoguan smelter using the flowsheet of ball milling neural leaching oxidizing roasting chloridizing distillation hydrolysis. 针对韶冶真空炉提锌产生的富锗渣 ，提出了“球磨 中性浸出 氧化焙烧 氯化蒸馏 水解”工艺回收其中的锗。