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The contents of dioxins compounds (PCDD/Fs) in the soil of certain hillock in Foshan City, Pear River Dalta were analyzed applying HRGC/HRMS. 应用高分辨气相色谱/高分辨质谱(HRGC/HRMS)对珠江三角洲佛山市某地山丘土壤中二类化合物(PCDD/Fs)含量进行了分析.